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Hollow fibre-supported liquid membrane extraction and LC-MS/MS detection for the analysis of heterocyclic amines in urine samples

Heterocyclic amines (HCAs) are potent mutagens/carcinogens to which humans are frequently exposed through the consumption of cooked meat and fish food. The effect of normal intake of HCAs and their role in the aetiology of human cancer is unknown. To some extent, limitations of the existing analytical methods in monitoring the low levels of HCAs in biological samples have hindered obtaining conclu

The Diary Weblog and the Traveling Tales of Diasporic Tourists

As has been commonly recognised, the Internet enables a transcendence of physical and national boundaries and therefore constitutes an ideal place for forging diasporic connections. There is no denying that the Internet has the potential to greatly affect how diasporic identities and senses of belonging are formed; the question is how, and in what online context? This article investigates a cluste

Hydrolysis of tri- and monoacylglycerol by lipoprotein lipase: evidence for a common active site

The relationship between triacylglycerol and monoacylglycerol hydrolyzing activities of purified rat heart lipoprotein lipase was studied using emulsified trioleoylglycerol and micellar or albumin-bound monooleoylglycerol as substrates. The maximal reaction rates obtained with the two substrates were similar (650 and 550 nmol of fatty acid released per min per mg of protein, respectively). Additio

Local Smoothing for the Backscattering Transform

An analysis of the backscattering data for the Schrodinger operator in odd dimensions n3 motivates the introduction of the backscattering transform [image omitted]. This is an entire analytic mapping and we write [image omitted] where BNv is the Nth order term in the power series expansion at v=0. In this paper we study estimates for BNv in H(s) spaces, and prove that Bv is entire analytic in vH(s

Activated Protein C Protein C Inhibitor Complex in Patients With Abdominal Aortic Aneurysms: Is It Associated With Diameter and Growth Rate?

Increased thrombin activation has been documented in patients with abdominal aortic aneurysm (AAA). APC-PCI complex, a new biological marker of thrombin generation, was measured in a population of 232 patients with AAA relative and a control group and the association between aneurysm size, growth rate and APC-PCI was studied. The patients were divided into cohorts according to the AAA diameter and

Symmetry-resolved x-ray absorption fine structure and resonant Auger-spectator-electron decay study of O 1s -> Rydberg resonances in O-2

A series of resonant Auger-electron spectra excited at selected photon energies across the O 1s -> Rydberg resonances in O-2 has been measured. Applying a spectator-electron shake relaxation model originally introduced for atomic resonant Auger-electron spectra, and using, to a large extent, the assignments for the core-excited resonances available from the literature, many of the observed spectat

High-frequency QRS electrocardiogram

The standard 12-lead electrocardiogram (ECG) is one of the most commonly used methods for diagnosing heart disease. Standard ECG is not always optimal, however, and new ECG methods can provide additional information. Analysis of high-frequency QRS components (HF-QRS) has been shown to increase the diagnostic performance of the ECG. Several investigators have studied HF-QRS in different cardiac con

Receptor binding properties of amperozide

The receptor pharmacology of amperozide was investigated with in vitro radioligand binding technique. Amperozide possessed a high affinity to the 5-HT2 receptors (Ki = 16.5 +/- 2.1 nM) and a moderate affinity to alpha 1-adrenergic receptors of rat cerebral cortical membranes (Ki = 172 +/- 14 nM). The affinity of amperozide for striatal and limbic dopamine D2 receptors was low and not significantly

Concentration and Fluxes of Dissolved Organic Carbon (DOC) in Three Norway Spruce Stands along a Climatic Gradient in Sweden

Leaching of dissolved organic carbon (DOC) from the forest floor and transport in soil solution into the mineral soil are important for carbon cycling in boreal forest ecosystems. We examined DOC concentrations in bulk deposition, throughfall and in soil solutions collected under the O and B horizons in three Norway spruce stands along a climatic gradient in Sweden. Mean annual temperature for the

Electron spectroscopy study of the initial stages of iron phthalocyanine growth on highly oriented pyrolitic graphite.

The nature of the intermolecular and substrate bonds of iron phthalocyanine adsorbed on highly oriented pyrolitic graphite has been investigated by x-ray photoelectron spectroscopy and x-ray absorption spectroscopy. We find that the molecules grow in a highly ordered fashion with the molecules essentially plane-parallel to the surface in both the mono- and multilayers. The spectra obtained on both

Vitamin D, parathyroid hormone and the metabolic syndrome in middle-aged and older European men

Objectives: Low serum 25-hydroxyviatmin D (25(OH)D) and elevated parathyroid hormone (PTH) levels have been linked to insulin resistance, the metabolic syndrome (MetS) and its components. Data in healthy, community-dwelling Europeans are lacking, and previous studies have not excluded subjects receiving drug treatments that may distort the relationship between 25(OH)D/PTH and MetS. The aim of our

Galectin-3 inhibits Schwann cell proliferation in cultured sciatic nerve

The production of galectin-3, a carbohydrate-binding mammalian lectin, is upregulated in Schwann cells after peripheral nerve injury in areas where Schwann cells proliferate. Here we tested if galectin-3 affected proliferation of Schwann cells in cultured sciatic nerve segments. Galectin-3 significantly decreased the number of bromodeoxyuridine-labelled Schwann cell nuclei. Neither lactose nor a s

Separation of coal-tar constituents from soil particles in a two-liquid-phase slurry system

An evaluation has been made of the capability of rapeseed oil to dissolve polycyclic aromatic hydrocarbon (PAH) crystals in a biphasic system and of its capability to extract PAHs from polluted soil in a two-liquid-phase (TLP) slurry system. Up to 220 g l(-1) of the crystalline hydrocarbons could be dissolved in the organic phase, indicating oil/water-partitioning coefficients of 10(5). When soil

A novel rating scale to predict maximal exercise capacity.

To predict maximal exercise capacity, we have developed the rating of perceived capacity (RPC) scale, based on metabolic equivalents (METs). MET values from 1 to 20 were listed on a progressive scale and linked to physical activities. Test subjects rated their perceived capacity by choosing the most strenuous activity and the corresponding MET value that they could sustain for 30 min. In order to

Unbiased auxiliary basis sets for accurate two-electron integral approximations

We propose Cholesky decomposition (CD) of the atomic two-electron integral matrix as a robust and general technique for generating auxiliary basis sets for the density fitting approximation. The atomic CD (aCD) auxiliary basis set is calculated on the fly and is not biased toward a particular quantum chemical method. Moreover, the accuracy of the aCD basis set can be controlled with a single param

Future changes in vegetation and ecosystem function of the Barents Region

The dynamic vegetation model (LPJ-GUESS) is used to project transient impacts of changes in climate on vegetation of the Barents Region. We incorporate additional plant functional types, i.e. shrubs and defined different types of open ground vegetation, to improve the representation of arctic vegetation in the global model. We use future climate projections as well as control climate data for 1981

Topas-based lab-on-a-chip microsystems fabricated by thermal nanoimprint lithography

We, present a one-step technology for fabrication of Topas-based lab-on-a-chip (LOC) microsysterris by the use of thermal nanoimprint lithography (NIL). The technology is demonstrated by the fabrication of two working devices: a particle separator and a LOC with integrated optics for absorbance measurements. These applications demonstrate the fabrication of millimeter to micrometer-sized structure

Persistent pollutants in a salmon population (Salmo salar) of the southern Baltic Sea

Persistent pollutants in an Atlantic salmon (Salmo salar) population spawning in a river of southern Sweden were investigated. The population was characterized by a high growth rate. Some males reached 20-30 kg after 3 to 4 years in the sea. The fat content of migrating salmon varied by one order of magnitude and was the most significant correlate of pollutant concentrations. No relationships were

Identification of the site in the cGMP-inhibited phosphodiesterase phosphorylated in adipocytes in response to insulin and isoproterenol

Stimulation of rat adipocytes with insulin and isoproterenol results in serine phosphorylation and activation of the adipocyte cGMP-inhibited phosphodiesterase (cGI PDE), events believed to be important in the antilipolytic action of insulin (Degerman, E., Smith, C.J., Tornqvist, H., Vasta, V., Manganiello, V.C., and Belfrage, P. (1990) Proc. Natl. Acad. Sci. U.S.A. 87,533-537). Here we demonstrat

The Prigogine-Herman kinetic model predicts widely scattered flow data at high concentrations

The classical derivation of a traffic stream model (e.g. speed/concentration relation) from the equilibrium solutions of the Prigogine–Herman kinetic equation invokes the nontrivial assumption that the underlying distribution of desired speeds is nonzero for vanishingly small speeds. In this paper we investigate the situation when this assumption does not hold. It is found that the Prigogine–Herma