Operando Characterization of Porous Nickel Foam Water Splitting Electrodes Using Near-Ambient Pressure X-ray Photoelectron Spectroscopy
This study presents a practical approach for characterizing industrial water-splitting nickel foam electrodes under both cathodic and anodic conditions by employing synchrotron radiation near-ambient pressure X-ray photoelectron spectroscopy (NAP-XPS). The in situ studies reveal quantitatively reduced and oxidized Ni species on the electrode surface by recording the Ni 2p3/2 signals after cycling
