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The structures of N-t-butyl-2-(diphenylphosphino)benzylammoniumchloride and N-t-butyl-2-(diphenylphosphino)benzylaminediacetatepalladium(II) have been determined by X-ray crystallography. The Pd-complex was prepared by treating palladiumdiacetate with N-t-butyl-2-(diphenylphosphino)benzylamine in CH2Cl2 for 4 h at room temperature. The organic compound crystallises in the monoclinic space group P2

Aim To investigate whether nurses could be a useful tool for improving the reporting rate of adverse drug reactions (ADRs). Furthermore, we wanted to study how physicians working at the study departments would respond to nurses as reporters of ADRs and if the reporting from the nurses affected the reporting rate from the physicians. Methods Three departments of internal medicine and one unit for o

The thermal reaction of Co film deposited on Si(111) surfaces by a high current filter metal vacuum arc (FMEVAD) system has been studied. After deposition the films were annealed over the 400-900 degrees C temperature range for 30 min. Rutherford backscattering spectrometry (RBS) was used to characterize the elemental depth distributions in the films subjected to different annealing temperatures.

We present an abundance analysis of the very metal-poor, carbon-enhancedstar CS 29497-030. Our results indicate that this unusually hot turnoffstar (Teff = 6650 K, log g = 3.5) has a metallicity [Fe/H] =-2.8, and exhibits large overabundances of carbon ([C/Fe] = +2.38),nitrogen ([N/Fe] = +1.88), and oxygen ([O/Fe] = +1.67). This star alsoexhibits a large enhancement in its neutron-capture elements

Excited states of Ga-65 and Ga-67 nuclei were populated through the C-12(Ni-58,alpha p) and C-12(Ni-58,3p) reactions, respectively, and investigated by in-beam gamma-ray spectroscopic methods. The NORDBALL array equipped with a charged particle ball and 11 neutron detectors was used to detect the evaporated particles and gamma rays. The level schemes of Ga-6.5.67 were constructed On the basis of g

This paper offers a method for quantifying the global exchange of (natural) space and (labor) time underlying the economic success of the British textile industry in the late 18th and early 19th century. Using historical statistics on inputs of land and labor embodied in cotton and wool production, respectively, estimates are made of the amount of British land and labor that were ‘saved’ by displa

The Internet Low Bit-rate Coder (iLBC) is now widely used for Voice over Internet Protocol (VoIP) applications. Unlike speech coders such as those based on Code Excited Linear Prediction (CELP), the iLBC achieves superior robustness to packet loss by avoiding inter-frame coding dependencies. While robustness to packet loss is essential, a VoIP codec should also possess the flexibility to change it

In a case-control study at two country hospitals in Sweden, 110 consecutive postmenopausal women (age 50-75) with distal radius fracture were examined with the DXA-technique, on the injured radius, lumbar spine, and the right hip within three weeks after the fracture occurrence. Data was compared with 55 age-matched controls from The Swedish Population Register. The incidence of osteoporosis accor

The complex [(IMesH2)(PPh2Cy)Cl2RuCHPh] was synthesised and shown to be an active catalyst in ring-closing metathesis of a diallylmalonate. Its phosphine exchange was investigated in C6D6 using magnetisation transfer 31P NMR spectroscopy and it was found to operate via a dissociative mechanism with k353 = 4.1 ± 0.9 s−1, ΔH‡ = 84 ± 10 kJ mol−1 and ΔS‡ = 4 ± 28 J mol−1 K−1.

The difference between the resolvents of two selfadjoint extensions of a certain symmetric operator A is described by Krein's resolvent formula. We will prove an analog of Krein's formula in a general framework, apply it to extensions theory, and give a straightforward proof of Krein's formula including the case that A is not necessarily densely defined. We will also present a modification of Krei

This work was conducted to study the potential of molecularly imprinted polymers (MIPs) for the removal of oestradiol at trace concentrations (1 ppm - 1 ppb). An MIP synthesised with 17 beta-oestradiol as template was compared to non-imprinted polymers (NIP) synthesised under the same conditions but without template, a commercial C18 extraction phase and granulated activated carbon. At 1 ppb,oestr

A Saccharomyces cerevisiae screening strain was designed by combining multiple genetic modifications known to improve xylose utilization with the primary objective of enhancing xylose growth and fermentation in xylose isomerase (XI)-expressing strains. Strain TMB 3045 was obtained by expressing the XI gene from Thermus thermophilus in a strain in which the GRE3 gene coding for aldose reductase was

Serum samples from patients referred for liver biopsy for investigation of suspected chronic liver disease (n = 286) and from healthy middle-aged volunteers (n = 445) were analyzed for markers of exposure to GB virus C/hepatitis G virus (GBV-C/HGV), hepatitis B virus and hepatitis C virus. GBV-C/HGV analyses included GBV-C/HGV PCR for detection of viremia and GBV-C/HGV enzyme-linked immunosorbent

Pretreatment of mixed softwoods with SO2 impregnation and steam for production of ethanol has been investigated. The optimal conditions, both for sugar yield and ethanol yield, to assess the effect of inhibitors formed in the pretreatment, have been determined. The parameters investigated were: SO2 concentration (1-6% (w/w) dry matter), temperature (190-230 degrees C) and residence time (2-15 min)

We present a model that explains the anomalous intensity ratios betweeneach of two very bright UV lines of Fe II at 2507 Å and 2509Å and its corresponding satellite line, observed in HST spectra ofa compact gaseous condensation (blob B) in the vicinity of the starprotect eta Car.The model is based on the assumption that the FeIItransitions have a substantial optical thickness, which varies as ares